Phase composition (XRD patterns) of the tested magnesium potassium phosphate bone cements with varying Mg/P, P/L ratios and MgO particle sizes
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The cement specimens, after hardening, were crushed and ground in a mortar and then analyzed by a Phillips X’Pert Pro X-ray diffractometer (Almelo, The Netherlands) using Cu-Kα radiation. Data were collected from 2θ = 20–50° with a step size of 0.02°, a 40 kV voltage and a 40 mA current. The phase identification has been undertaken using HighScore Plus software with the International Centre for Diffraction Data (ICDD) database.




