Ether formation between 1 and 2.
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a)Reaction conditions: 30 mL THF, 0.972 mmol 1, 1.94 mmol 2, 9.72 mmol NaH; reflux (ca. 339 K); reaction time: 12 h. b) Reaction conditions: 30 mL THF, 0.486 mmol 1, 0.972 mmol 2, 4.86 mmol NaH; reflux (ca. 339 K); reaction time: 12 h. c) Isolated yields.
创建时间:
2015-12-02



