Synthesis and X-ray Crystal Structure of [(C5Ph5)CrCl(μ-Cl)2Tl]2: An Example of the Rare M−X−TlI Linkage (X = Halide)
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https://figshare.com/articles/dataset/Synthesis_and_X-ray_Crystal_Structure_of_C_sub_5_sub_Ph_sub_5_sub_CrCl_-Cl_sub_2_sub_Tl_sub_2_sub_An_Example_of_the_Rare_M_X_Tl_sup_I_sup_Linkage_X_Halide_/12074298
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Reaction of solid TlCl with [(C5Ph5)CrCl(μ-Cl)]2 in CH2Cl2 solvent yields the dimeric complex [(C5Ph5)CrCl(μ-Cl)2Tl]2 in 80% isolated yield. The C5H5 and C5Me5 analogues do not react with TlCl, suggesting a steric basis for the reaction of the C5Ph5 material.
创建时间：
2007-09-10
