Polymorphism in 4-Methoxy-3-nitrobenzaldehyde
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https://figshare.com/articles/dataset/Polymorphism_in_4_Methoxy_3_nitrobenzaldehyde/3077251
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资源简介:
Two of the three earlier reported polymorphic forms of 4-methoxy-3-nitrobenzaldehyde have been reinvestigated
and fully characterized by a variety of methods including variable temperature powder X-ray diffraction, vibrational spectroscopy
(infrared and Raman), calorimetry (differential scanning calorimetry, DSC), and optical microscopy. Differences of DSC thermograms,
which were carried out with different cooling rates, suggest a thermodynamic/kinetic competition in the crystallization from the
melt. The crystal structures of these two forms have been solved, one by single-crystal methods and the second from synchrotron
powder diffraction.
创建时间:
2016-03-01



