Quantitative phase analysis of powder X-ray diffraction patterns of Ti3C2Tz MXene synthesis products

Rietveld refinement was performed on powder diffraction patterns of a triphasic system, where one phase constitutes an internal standard, to be able to quantify the proportion of product (Ti3C2 MXene) and reactant (Ti3AlC2 MAX phase) present after a synthesis trial. Synthesis trial parameters are determined in a Design of Experiments (DoE) screening design.See file 2022-12-06-Quantitative-Phase-Analysis-QPA-of-MXene-synthesis-product-PXRD-patterns.pdf for full dataset details.