Organometallic Compounds of the Lanthanides. 179. Synthesis and Structural Characterization of a Mixed Alkyl (Benzhydryl, Trimethylsilylmethyl) Lutetium Complex
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https://figshare.com/articles/dataset/Organometallic_Compounds_of_the_Lanthanides_179_Synthesis_and_Structural_Characterization_of_a_Mixed_Alkyl_Benzhydryl_Trimethylsilylmethyl_Lutetium_Complex/3223834
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The reaction of LuCl3(THF)3 with 2 equiv of LiCH2SiMe3 and 1 equiv of KCHPh2 (1) affords Lu(CH2SiMe3)2(CHPh2)(THF)2 (2). X-ray structural analyses show the benzhydryl unit to be planar in 1, but bent in 2.
创建时间：
2016-05-05
