In-situ Solid-state NMR Spectra of Urea and 1,10-Decanediol Co-Crystallizing

This project used in-situ solid-state NMR to study the crystallization of urea and 1,10-decanediol from methanol. Two solid products were formed. A urea inclusion compound appeared first, followed by a co-crystal.The data was acquired on a Bruker AVANCE III NMR spectrometer (20.0 T; 13C Larmor frequency, 213.8 MHz) at the U.K. High-Field Solid-State NMR Facility.The text files contain the real and imaginary parts of the 2D dataset. They were generated by the Bruker software "TopSpin".The data can be viewed in any text editor and plotted in Excel or other similar programs. Mathematica was used to process the data for publication.