Hydrolysis data for bis(4-cyanophenyl) phenyl phosphate

This dataset obtained from hydrolysis process of bis(4-cyanophenyl) phenyl phosphate (CPP). The dataset contains raw NMR-spectroscopy data of CPP and products of hydrolysis (can be open with e.g. ACDLabs Spectrus processor) as 1H, 13C, 31P NMR free induction decays (FID), raw HPLC chromatograms including initial chromatograms of CPP, 4-cyanophenol and phenol, and chromatograms obtained during hydrolysis study (.pdf). Hydrolysis was carried out under pH 4, 7, 10 and at temperatures of 25, 35, 50, 60 and 80°C. Two series of aliquots were selected from the reaction mixture in certain time periods to obtain the average values of the peak areas in the chromatograms.本数据集源自双(4-氰基苯基)苯基磷酸酯（bis(4-cyanophenyl) phenyl phosphate，CPP）的水解反应过程。数据集包含CPP及其水解产物的原始核磁共振（Nuclear Magnetic Resonance，NMR）波谱数据，可通过ACDLabs Spectrus处理器等软件打开，具体包括¹H、¹³C、³¹P NMR自由感应衰减（free induction decays，FID）数据；同时涵盖原始高效液相色谱（High Performance Liquid Chromatography，HPLC）谱图，其中包含CPP、4-氰基苯酚及苯酚的初始色谱图，以及水解研究过程中获取的色谱谱图（存储为.pdf格式）。本次水解实验分别在pH值为4、7、10的条件下，以及25℃、35℃、50℃、60℃、80℃的温度梯度中开展。研究人员在特定时间区间从反应混合液中选取两组等分试样，以获取色谱图中峰面积的平均值。