Crystallographic Characterisation of Organolithium and Organomagnesium Intermediates in Reactions of Aldehydes and Ketones

The dataset contains four files: 1.NMR data (zip file) 2.Infrared data (zip file) 3.Crystallographic information file (X-ray crystallographic data) 4.CheckCIF (for X-ray crystallographic data) This data relates to the research reported in the manuscript "Crystallographic Characterisation of Organolithium and Organomagnesium Intermediates in Reactions of Aldehydes and Ketones", carried out in connection with the EPSRC DTP award "EP/T517938/1". Please note that the NMR data contained in file 1 requires a specialist program such as Topspin or Mestrelab and the CIF file (file 3) requires a program such as Diamond or Mercury to view.