Self-Assembly of a Nanosized, Saddle-Shaped, Solution-Stable Polyoxometalate Anion Built from Pentagonal Building Blocks: [H<sub>34</sub>W<sub>119</sub>Se<sub>8</sub>Fe<sub>2</sub>O<sub>420</sub>]<sup>54−</sup>
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Precise control of the “one-pot” reaction conditions is employed for the assembly of a nanosized 2.8 nm cluster, [H34W119Se8Fe2O420]54− (1a), which is templated using eight selenite units and two iron(III) centers. Not only is this cluster characterized structurally using X-ray crystallography, it is the largest polyoxotungstate to be observed intact in solution using ESI-MS, with a molecular mass of ca. 30 000 Da.
创建时间：
2016-02-24
