Quantitative three-dimensional local order analysis of nanomaterials through electron diffraction

Diffraction data for Yttrium Stabilized Zirconia Zr0.82Y0.18O1.91

Electron diffraction data:

FEI Tecnai G2 microscope

200 keV electrons

Cheetah detector (ASI, 512 x 512 pixel)

Condenser Aperature 10 micrometer, spot size 9

Exposure 1.512 s / frame, rotation 0.4 deg/frame

raw data was processed with PETS2 (http://pets.fzu.cz/)

X-ray diffraction data:

Rigaku Syneergy S diffractometer

Eiger 1M Detector, energy discriminating threshold 17.4 keV

Mo K-alpha radiation

120 s exposure time, 0.5 deg/frame

Raw data can be processed with CrysAlisPro (https://www.rigaku.com/products/crystallography/crysalis)

Neutron diffraction data:

D19 ILL, Grenoble

0.95 A wavelength

80 s exposure time, 0.1 deg/frame

Raw data can be accessed at doi:10.5291/ILL-DATA.5-13-277 and processed with the Instrument software Int3D (https://www.ill.eu/users/instruments/instruments-list/d19/software)

Reciprocal space reconstructions and 3D-DeltaPDF maps

Provided in .h5 format and can be vizualized e.g. with DISCUS (https://github.com/tproffen/DiffuseCode/releases) or DensityViewer (https://github.com/aglie/DensityViewer/releases/)