Quantitative three-dimensional local order analysis of nanomaterials through electron diffraction

Diffraction data for Yttrium Stabilized Zirconia Zr0.82Y0.18O1.91 Electron diffraction data: FEI Tecnai G2 microscope 200 keV electrons Cheetah detector (ASI, 512 x 512 pixel) Condenser Aperature 10 micrometer, spot size 9 Exposure 1.512 s / frame, rotation 0.4 deg/frame raw data was processed with PETS2 (http://pets.fzu.cz/) X-ray diffraction data: Rigaku Syneergy S diffractometer Eiger 1M Detector, energy discriminating threshold 17.4 keV Mo K-alpha radiation 120 s exposure time, 0.5 deg/frame Raw data can be processed with CrysAlisPro (https://www.rigaku.com/products/crystallography/crysalis) Neutron diffraction data: D19 ILL, Grenoble 0.95 A wavelength 80 s exposure time, 0.1 deg/frame Raw data can be accessed at doi:10.5291/ILL-DATA.5-13-277 and processed with the Instrument software Int3D (https://www.ill.eu/users/instruments/instruments-list/d19/software) Reciprocal space reconstructions and 3D-DeltaPDF maps Provided in .h5 format and can be vizualized e.g. with DISCUS (https://github.com/tproffen/DiffuseCode/releases) or DensityViewer (https://github.com/aglie/DensityViewer/releases/)