Oxidation of Ni-ECp* Complexes: Stable Open-Shell NiI Cations [Ni(ECp*)n(PPh3)4–n]+ (n = 2, 4; E = Al, Ga)
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https://figshare.com/articles/dataset/Oxidation_of_Ni_ECp_Complexes_Stable_Open_Shell_Ni_sup_I_sup_Cations_Ni_ECp_sub_i_n_i_sub_PPh_sub_3_sub_sub_4_i_n_i_sub_sup_sup_i_n_i_2_4_E_Al_Ga_/2120263
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Uncommon NiI cationic complexes were synthesized by treating [Ni(ECp*)2(PPh3)2] (E = Al, Ga; Cp* = pentamethylcyclopentadienyl) with 1 equiv of [FeCp2][BAr4F]. All compounds have been prepared readily in high yield. The paramagnetic compounds were characterized by single-crystal X-ray crystallography, mass spectrometry, elemental analysis, magnetic susceptibility, and electron paramagnetic resonance spectroscopy.
创建时间：
2016-02-12
