AMPHIBIAN CSIC experimental data insitu exsitu PXRD NPD

The different datasets are divided in folders as follows: 1. In situ experiments. The article is based on 7 different in situ experiments: a. 400C_5mLmin_fr10; b. 400C_10mLmin_fr23; c. 400C_20mLmin_fr6; d. 400C_30mLmin_fr12; e. 300C_10mLmin_fr4; f. 350C_10mLmin_fr18; g. 500C_10mLmin_fr9. (Due to space limitations, only the data corresponding to the experiment c were uploaded to this repository. The remaining data are accessible through private communication with Cecilia Granados-Miralles, [e-mail]). The folder “c_400C_20mLmin_fr6” contains in situ PXRD data (time resolution=5 s) collected during reduction at the temperature and gas flow indicated in the folder name (i.e. 400C_20mLmin stands for 400 °C and 20 mL/min). The temperature indicated in the file names is the set temperature but the sample temperature is the indicated in the folder name (i.e. Tset430 led to a sample temperature of 400 °C). Heating started on the frame indicated in the folder name (i.e. fr6 stands for frame 6). This folder contains 2D-diffraction images in *.tif format, which may be opened with the Python-based program for on-the-fly data processing and exploration of two-dimensional X-ray diffraction area detector data, available for free download at http://www.clemensprescher.com/programs/dioptas.