3DED data of lanthanum hexaboride

3DED data of commerically obtained lanthanum hexaboride were collected using continuous rotation in selected area mode. The table below summarizes data collection parameters. General information Project Project label Sample label LaB6 Collection site University of Southampton, NCS Instrumental Instrument Rigaku XtaLAB Synergy-ED, electron diffractometer Radiation source LaB6 Accelerating voltage [kV] 200 Wavelength [Å] 0.02510 Probe type Parallel beam Beam diameter Beam convergence Parallel beam Detector Rigaku HyPix-ED, hybrid pixel array detector Number of pixels in the image 775 x 385 Pixel size [µm] 100 Hardware binning 1 Sample description Name lanthanum hexaboride Chemical composition La B6 Sample source commercial (Sigma Aldrich 241857) Grid Agar Scientific holey carbon coated copper grid 200 mesh Sample preparation solid sample gently ground and dispersed between microscopy glass slides, grid tapped on solid Sample holder JEOL standard TEM holder with high tilt retainer Experimental Data type Electron diffraction data - 3DED Data collection method continuous rotation - cRED Collection temperature [K] rt Software Software used for the data collection CrysAlisPro 1.171.43.111a Software used for processing CrysAlisPro 1.171.43.119a Files and data formats Image folders ./frames/xxx.rodhypix./frames/PETS_exp_701/frames/xxx.tiff Image format .rodhypix (Rigaku proprietary image format).tiff (16bit, converted with CrysAlisPro 1.171.43.119a) Additional files CrysAlisPro input files:./expinfo/./CrysalisExpSettings.ini./exp_701.par./exp_701.run./new.ccd PETS2 (http://pets.fzu.cz/) input file:./frames/PETS_exp_701/exp_701.pts2 Crystal Image:./exp_701_microed_grain_snapshot.jpg