Synthesis of a Masked 2,3-Diaminoindole
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https://figshare.com/articles/dataset/Synthesis_of_a_Masked_2_3-Diaminoindole/4272986
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资源简介:
A three-step
synthesis of masked 2,3-diaminoindole 1 from 2-iodo-3-nitro-1-(phenylsulfonyl)indole
(2) has been developed. Treatment of 1 with
trifluoroacetic acid generates the unstable 2,3-diamino-1-(phenylsulfonyl)indole
(3), which can be trapped with α-dicarbonyl compounds
to afford 5H-pyrazino[2,3-b]indoles 7–10.
创建时间:
2016-12-01



