Single-crystal 3D electron diffraction dataset for sodium oxalate
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https://repod.icm.edu.pl/citation?persistentId=doi:10.18150/P1SIJH
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资源简介：
Electron diffraction dataset collected from sodium oxalate (Sigma-Aldrich) micro crystals obtained by slow evaporation from water.Microscope: Thermo Fisher Scientific 200kV Glacios Transmission Electron Microscope (Cryomicroscopy and Electron Diffraction Core Facility at the Centre of New Technologies, University of Warsaw, Poland)Camera: Ceta-D camera (bin 2x2, rolling shutter, noise reduction mode)Collection Software: EPU-D (Thermo Fisher), SMV formatCollection Parameters: 200keV, -193C, 50um C2, gun lens 8, spot size 11, extraction voltage 3850V, parallel beam, beam diameter ~1.7 um, beam stop inserted, oscillation per frame 0.4 deg, 0.5 s exposure time, tilt speed 0.8 deg/s, rotation -60 to +60 degGrid: lacey carbon Cu 200 mesh glow discharged for 60s at 25mASample: sodium oxalate
提供机构：
RepOD
创建时间：
2025-06-15
