3DED raw data for "A flexible copper MOF as a carboxylate-selective crystalline sponge for structure solution using X-ray and electron diffraction"

Raw 3D ED data for crystal structures included in the title publication (https://doi.org/10.1039/D5SC05651A). Collection site University of Southampton, NCS Sample labels CCDC2415257, CCDC2415258, CCDC2415259 Instrumental Instrument Rigaku XtaLAB Synergy-ED, electron diffractometer Radiation source LaB6 Accelerating voltage [kV] 200 Wavelength [Å] 0.0251 Probe type Parallel beam Beam diameter Beam convergence Parallel beam Detector Rigaku HyPix-ED, hybrid pixel array detector Number of pixels in the image 775 x 385 Pixel size [µm] 100 Hardware binning 1 Experimental Data type Electron diffraction data - 3DED Data collection method continuous rotation - cRED Collection temperature [K] 175 Software Software used for the data collection CrysAlisPro Software used for processing CrysAlisPro Files and data formats Image folders ./frames/xxx.rodhypix./frames/TIFF/xxx.tiff Image format .rodhypix (Rigaku proprietary image format).tiff (32bit, converted with CrysAlisPro 1.171.44.86a) Additional files CrysAlisPro input files:./expinfo/./CrysalisExpSettings.ini./exp_XXX.par./exp_XXX.run./new.ccd