Simple Synthesis of an Allenylidene Heptavalent Rhenium(<i>d</i><sup>0</sup>) Complex
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This paper reports a simple way to synthesize an allenylidene rhenium(VII) complex. The diimido adamantyl-thiolato allenylidene rhenium(VII) complex 2 was obtained through a metathetical reaction of phosphonioalkylidyne rhenium complex 1 with diphenylketene and also structurally analyzed with X-ray diffraction. Complex 2 is the first d0 allenylidene complex with structure information.
创建时间：
2016-05-06
