Design and optimization of 3D-printed packed bed reactor for continuous catalytic hydrogenation of nitroaromatic compounds

The colletion contains a set of data related to the design and optimization of packed bed reactor (PBR) for the continous reduction of 4-nitrophenol. The development of PBR involved 3D-printing using stereolitography as well as the initial assessment of process parameters. The PBR contained heterogenous catalyst loaded with rhenium nanoparticles, that enabled carrying out effective hydrogenation in a flow-mode system.The research was carried out within Sonata 16 project (UMO-2020/39/D/ST8/01352) granted by National Science Center (Poland). Aim of the project is to develop new generation of catalytical-separation technology for the simultaneous hydrogenation of nitroaromatic compounds and extraction of resulting from the process aromatic amines.The set of data contains:Raw HRTEM/HAAFD images and EDX maps obtained during transmission electron microscopy analysis.UV-Vis spectra recorded during catalytic reduction of 4-nitrophenol.XPS spectra of the samples containing rhenium nanoparticles.3D STL models with the column design