Optimised recovery of double-base smokeless powder residues analysed by TV-SPME/GC-MS

This dataset was collected by Georgina Sauzier at Indiana University-Purdue University, Indianapolis in 2015 as part of a PhD exchange placement, as described in the linked article. Simulated smokeless gunpowder residues were analysed using total vaporisation (TV)-SPME/GC-MS as part of a central composite design. Optimised parameters for recovery of the target components were then tested using real residues generated from a pipe bomb detonation.

Peak areas were integrated using Thermo Xcalibur v2.0.7. The central composite design was created and analysed using Design Expert v10.

本数据集由乔治娜·索齐耶（Georgina Sauzier）于2015年在印第安纳大学-普渡大学印第安纳波利斯分校（Indiana University-Purdue University, Indianapolis）收集，系其博士交换访学项目的一部分，相关细节详见所附链接文章。研究采用总挥发（Total Vaporisation, TV）-固相微萃取（Solid Phase Microextraction, SPME）/气相色谱-质谱（Gas Chromatography-Mass Spectrometry, GC-MS）联用技术对模拟无烟火药残留物进行分析，实验设计采用中心复合设计（Central Composite Design）。随后，针对目标组分回收率的优化参数，使用管道炸弹爆炸产生的真实残留物开展了验证测试。
峰面积积分采用赛默飞Xcalibur v2.0.7软件完成；中心复合设计的构建与分析则通过Design Expert v10软件实现。