遇见数据集

3D ED raw data for "Understanding the Solid-State Landscape of PROteolysis TArgeting Chimeras"

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Zenodo2025-07-24 更新2026-05-26 收录
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3D ED data for the crystal structure in the title publication (https://doi.org/10.1021/jacs.5c07977). Data were collected using continuous rotation in selected area mode. The table below summarizes generic data collection parameters for the data collection. Collection site University of Southampton, NCS/NEDF Sample label(s) 2024NCS0774 Crystal structure deposit CSD 2445862 Instrumental Instrument Rigaku XtaLAB Synergy-ED, electron diffractometer Radiation source LaB6 Accelerating voltage [kV] 200 Wavelength [Å] 0.02510 Probe type Parallel beam (SAED) Beam convergence Parallel beam Detector Rigaku HyPix-ED, hybrid pixel array detector Number of pixels in the image 775 x 385 Pixel size [µm] 100 Hardware binning 1 Sample description Name AZ1 Form1 Chemical composition C49H63FN10O3 Sample source Synthesis Grid Holey carbon coated copper grid, 200 mesh (Agar Scientific) Sample preparation Sample ground between glass slides, grid dabbed, plunged in liquid nitrogen, cryo transfer @ 175 K Sample holder GATAN Elsa cryo-transfer holder 698 Experimental Data type Electron diffraction data - 3D ED Data collection method Continuous rotation - cRED Collection temperature [K] 175 Software Software used for the data collection CrysAlisPro 1.171.44.78a Software used for processing CrysAlisPro 1.171.44.79a Files and data formats Image folders ./frames/xxx.rodhypix./frames/TIFF/xxx.tiff Image format .rodhypix.tiff (converted with CrysAlisPro) Additional files CrysAlisPro files: ./expinfo/./expinfo/exp_XXXX_datacoll.ini ./plots_dc.plots_dc/exp_XXX_hypix.dat.plots_dc/exp_XXX_Jeol_MicroED.dat.plots_dc/exp_XXX_primarybeam.dat.plots_dc/exp_XXX_primarybeam_0.jpg ./CrysalisExpSettings.ini./exp_XXX.par./exp_XXX.run./new.ccd Grain snapshots files: ./exp_XXXX_microed_grain_snapshot.rodhypix./exp_XXXX_microed_grain_snapshot.tiff./exp_XXXX_microed_post_snapshot.rodhypix./exp_XXXX_microed_post_snapshot.rodhypix

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2025-05-07
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