X-ray data for 4, 8-dithiatricyclo[7.2.1.0^(3,10)]dodecane

The crystal structure of 4, 8-dithiatricyclo[7.2.1.03,10]dodecane was obtained. The structure was solved by direct methods. A total of 9 atoms were located from the E-map. The remaining atoms were located in succeeding difference Fourier syntheses. Hydrogen atoms were included in the refinement but restrained to ride on the atom to which they are bonded.

已成功解析得到4,8-二硫杂三环[7.2.1.03,10]十二烷的晶体结构。该结构通过直接法完成解析。从电子密度图（E-map）中共计定位出9个原子，剩余原子则通过后续的差值傅里叶合成（difference Fourier syntheses）完成定位。氢原子参与了结构精修，但采用骑乘式约束，使其固定于其所键合的原子上。