In situ FTIR, EXAFS and HR-STEM data for Pd/TiO2 samples under red-ox conditions

Files Pd_photo-oxidation.xmu.dat and Pd_dep-oxidation.xmu.dat contain the sequence of X-ray absorption spectra during starting from the pre-reduced state (after reduction in H2) during heating in O2 from 50 to 400 for Pd_photo and Pd_dep samples, respectively (synthesized using photodeposition and deposition-precipitation methods). The last two columns in each file correspond to the as-synthesized state of the corresponding sample (before reduction in hydrogen) and reference palladium foil. 

Pd_photo.ftir.dat and Pd_dep.ftir.dat contain the sequence of the FTIR spectra for the same samples taken at room temperature after sending 35 mbar of CO on pre-oxidized samples.

Pd_photo_220_O2_80kV.wmv shows the evolution of Pd_dep sample under O2 at 220 C, visualized by in situ HR-STEM microscope.