Determination of the experimental minimal formula of metal-organic frameworks
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The .pxp documents contain the experimental data of the figures in the manuscript and SI and they can be opened/edited with the software IGOR Pro 6.3 or higher. Figure 2: TGA and 1H NMR data of UiO-66(Zr) and MOF-808(Zr). Figure 3: 1H NMR spectra of MOF-808(Zr) digested in 1M NH4HCO3, acquired at two different relaxation delay. Figure 4: UV–vis absorption spectra of MOF-808 sample after digestion in base and addition of the reagents for the chloride ion test. Figure S1 - S53: Figures from Supporting Information.
所有.pxp格式文件包含论文手稿及补充材料(Supporting Information,简称SI)中所有配图对应的实验数据,可通过IGOR Pro 6.3及更高版本软件打开或编辑。 图2:UiO-66(Zr)与MOF-808(Zr)的热重分析(Thermogravimetric Analysis,简称TGA)及氢核磁共振(Proton Nuclear Magnetic Resonance,简称¹H NMR)数据。 图3:MOF-808(Zr)在1 mol/L碳酸氢铵(NH₄HCO₃)中消解后得到的¹H NMR谱图,采用两种不同弛豫延迟时间采集得到。 图4:MOF-808样品经碱消解并添加用于氯离子检测的试剂后的紫外-可见(Ultraviolet-Visible,简称UV-Vis)吸收光谱。 图S1~S53:补充材料中的配图。



