Primary data for the manuscript provisionally titled, "Azide-Alkene Cycloaddition and Visible-Light mediated Wolff Rearrangement of Sugar Enones"

NMR data for all new compounds including 1H and 13C FID files and mass spectra. NMR files can be opened using Bruker Topspin software or Spinworks.本数据集包含所有全新化合物的核磁共振波谱（Nuclear Magnetic Resonance, NMR）数据，涵盖氢谱（¹H）与碳谱（¹³C）的自由感应衰减（Free Induction Decay, FID）文件以及质谱数据。此类核磁共振文件可通过布鲁克Topspin软件或Spinworks软件打开。