Thermoporometry analysis of silica and carbon materials: comparison of calibration method and delta layer width determination approach

This dataset contains raw experimental data used for the thermoporometry (TPM) characterization of mesoporous silica (S1–S3) and carbon materials (C1–C2). The dataset includes differential scanning calorimetry (DSC) curves of frozen water melting in porous structures and nitrogen physisorption isotherms measured at 77 K. The data enable independent evaluation of pore size distributions using different TPM approaches, including calibration-based and δ-layer methods, as described in the associated publication.本数据集包含用于介孔二氧化硅（S1–S3）与碳材料（C1–C2）的热孔隙率法（thermoporometry, TPM）表征的原始实验数据。数据集涵盖了多孔结构内冻结水熔融的差示扫描量热法（differential scanning calorimetry, DSC）曲线，以及在77 K下测得的氮气物理吸附等温线。如相关出版物所述，本数据可通过不同的TPM方法（包括基于校准法与δ层法）独立评估孔径分布。