In Crystallo Lattice Adaptivity Triggered by Solid-Gas Reactions of Cationic Group 7 Pincer Complexes
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https://zenodo.org/record/8212886
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资源简介：
3DED/microED datasets of [Mn(iPr-PONOP)(CO)3][BArF4] collected using a Thermo Fisher Scientific Glacios microscope equipped with a Ceta-D Camera associated with the publication "In Crystallo Lattice Adaptivity Triggered by Solid-Gas Reactions of Cationic Group 7 Pincer Complexes" published in Chem. Commun.
Data collection details:
200kV, nanoprobe, gun lens 8, spot size 11, 30 µm C2 aperture. Illuminated area was ~1 µm. Under these conditions flux is 0.06 – 0.07 e-/Å^2/s. Camera length calibrated from Al powder was 958.5 mm. Data acquired using EPU-D with following settings: 2x binning, 2°/s, 0.5s exposure, rolling shutter, noise reduction mode enabled.
MRC format images can be processed with DIALS using the FormatMRC dxtbx format (distributed with DIALS from version 3.5 onwards), use goniometer.axes=1,0,0.
创建时间：
2023-08-08
