In Crystallo Lattice Adaptivity Triggered by Solid-Gas Reactions of Cationic Group 7 Pincer Complexes

3DED/microED datasets of [Mn(iPr-PONOP)(CO)3][BArF4] collected using a Thermo Fisher Scientific Glacios microscope equipped with a Ceta-D Camera associated with the publication "In Crystallo Lattice Adaptivity Triggered by Solid-Gas Reactions of Cationic Group 7 Pincer Complexes" published in Chem. Commun. Data collection details: 200kV, nanoprobe, gun lens 8, spot size 11, 30 µm C2 aperture. Illuminated area was ~1 µm. Under these conditions flux is 0.06 – 0.07 e-/Å^2/s. Camera length calibrated from Al powder was 958.5 mm. Data acquired using EPU-D with following settings: 2x binning, 2°/s, 0.5s exposure, rolling shutter, noise reduction mode enabled. MRC format images can be processed with DIALS using the FormatMRC dxtbx format (distributed with DIALS from version 3.5 onwards), use goniometer.axes=1,0,0.