FTIR and NMR spectra of impurified and purified acrylonitrile (AN) (Original data)
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This dataset contains FTIR and NMR spectra for the successful purification of acrylonitrile (AN) monomer by a simple column technique which is related to our published paper with DOI 10.3390/polym13040660 1. FTIR_Non Pure AN_ Raw Data (Excel)<br> 2. FTIR_ Pure AN_ Raw Data (Excel)<br> 3. SigmaPlot FTIR_ Pure AN_ Raw Data<br> 4. SigmaPlot FTIR_ Non Pure AN_ Raw Data<br> 5. Pure AN_1H (1)<br> 6. Pure AN_1H (2)<br> 7. Pure AN_13C(1)<br> 8. Pure AN_13C (2)<br> 9. Non Pure AN_1H (1)<br> 10. Non Pure AN_1H (2)<br> 11. Non Pure AN_13C (1)<br> 12. Non Pure AN_13C (2) In fact, As known, purification is of the utmost significance in any chemistry process. Besides, eliminating impurities enhances the quality and standard of the product. The primary method for monomer purification, like acrylonitrile (AN), is the distillation technique. However, this technique is unsafe and hard to set up or handle. A straightforward, risk-free, and low-cost method like the column technique resolves these issues. Therefore, the data will be helpful in numerous applications, especially in polymerization reactions that require the removal of inhibitors before the polymerization initiation process.
本数据集包含通过简易柱层析技术成功提纯丙烯腈(acrylonitrile, AN)单体所获得的傅里叶变换红外光谱(FTIR)与核磁共振波谱(NMR),相关研究已发表于DOI为10.3390/polym13040660的学术论文。 1. 未纯化丙烯腈傅里叶变换红外原始数据(Excel格式) 2. 纯丙烯腈傅里叶变换红外原始数据(Excel格式) 3. 纯丙烯腈傅里叶变换红外原始数据(SigmaPlot格式) 4. 未纯化丙烯腈傅里叶变换红外原始数据(SigmaPlot格式) 5. 纯丙烯腈¹H核磁共振谱图(1) 6. 纯丙烯腈¹H核磁共振谱图(2) 7. 纯丙烯腈¹³C核磁共振谱图(1) 8. 纯丙烯腈¹³C核磁共振谱图(2) 9. 未纯化丙烯腈¹H核磁共振谱图(1) 10. 未纯化丙烯腈¹H核磁共振谱图(2) 11. 未纯化丙烯腈¹³C核磁共振谱图(1) 12. 未纯化丙烯腈¹³C核磁共振谱图(2) 事实上,众所周知,纯化工序在各类化学工艺中均具备至关重要的意义。去除杂质可显著提升产品的品质与标准化水平。传统上,丙烯腈等单体的纯化主要采用蒸馏工艺,但该方法存在安全隐患,且搭建与操作难度较大。而柱层析技术这类简便、安全且低成本的纯化方案,则可有效解决上述问题。因此,本数据集可应用于诸多研究场景,尤其适用于聚合反应启动前需脱除抑制剂的聚合反应研究。



