Tailoring the adhesion of electrophoretic chitosan/bioactive glass coatings by the combined surface pre-treatments of Ti substrates

This record contains all files generated in the preparation process of the following publication: Agnieszka Kowalczyk, Agata Sotniczuk, Donata Kuczyńska-Zemła, Jarosław Pura, Zhiyan Xu, Aldo R. Boccaccini, Halina Garbacz,"Tailoring the adhesion of electrophoretic chitosan/bioactive glass coatings by the combined surface pre-treatments of Ti substrates", submitted to Surface and Coatings Technology. Designations: Ti_G2 - Titanium Grade 2 G - sample grinded on #600 grit abrasive paperSP - sample shot-peened with 90-150 µm shots, under pressure of 0.5 MPaE - sample etched SP+E_HF - sample shot-peened with 90-150 µm shots, under the pressure of 0.5 MPa and etched in the hydrofluoric solution SP+E_NaOH - sample shot-peened with 90-150 µm shots, under the pressure of 0.5 MPa and etched in the sodium hydroxide solutionSP+E_HF_NaOH - sample shot-peened with 90-150 µm shots, under the pressure of 0.5 MPa and etched first in the hydrofluoric solution and then in sodium hydroxide EPD - samples coated with chitosan/bioglass coatingADH - samples coated with chitosan/bioglass coating after conducted adhesion testSBF - samples after bioactivity test in Simulated Body Fluid (SBF) solutionSEM - Scaning Electron Microscopy EDS - Energy Dispersive Spectroscopy Folders content: Corrosion - contains files with data of corrosion resistance, obtained during electrochemical tests FTIR - contains files obtained from Fourier Transform Infrared Spectroscopy analysis of chitosan/bioglass coating Roughness - contains files from topography analysis obtained using optical profilometer for various scan areas SEM - contains folders with images of samples surfaces from Scanning Electron Microscopes. Subfolders: Adhesion - contains SEM images of samples coated with chitosan/bioglass coatings after tape test Bioactivity test - contains SEM images and EDS analysis of samples coated with chitosan/bioglass coatings after bioactivity test in SBF Coatings - contains SEM images of chitosan/bioactive glass coatings deposited on different substrates Substrate - contains SEM images of titanium substrate after various surface modifications Wettability - contains files with data obtained from wettability tests XRD - contains files with data obtained from X-ray spectroscopy analysis This research was supported financially by the National Science Centre, Poland under the grant OPUS 23 [2022/45/B/ST5/03398].本数据集包含为下述学术论文筹备过程中生成的全部文件： 阿格涅什卡·科瓦尔奇克（Agnieszka Kowalczyk）、阿加塔·索特尼丘克（Agata Sotniczuk）、多纳塔·库琴斯卡-热姆拉（Donata Kuczyńska-Zemła）、雅罗斯瓦夫·普拉（Jarosław Pura）、徐芝艳（Zhiyan Xu）、阿尔多·R·博卡奇尼（Aldo R. Boccaccini）、哈利娜·加尔巴茨（Halina Garbacz），论文题为《通过钛基底联合表面预处理调控电泳沉积壳聚糖/生物活性玻璃涂层的粘附性能》，已投稿至《Surface and Coatings Technology》（《表面与涂层技术》）。 样品代号说明： Ti_G2：2级钛（Titanium Grade 2） G：经#600粒度砂纸研磨的试样 SP：采用90~150μm弹丸、0.5MPa压力进行喷丸处理的试样 E：经蚀刻处理的试样 SP+E_HF：采用90~150μm弹丸、0.5MPa压力喷丸后，于氢氟酸溶液中蚀刻的试样 SP+E_NaOH：采用90~150μm弹丸、0.5MPa压力喷丸后，于氢氧化钠溶液中蚀刻的试样 SP+E_HF_NaOH：采用90~150μm弹丸、0.5MPa压力喷丸后，依次经氢氟酸溶液、氢氧化钠溶液蚀刻的试样 EPD：涂覆壳聚糖/生物活性玻璃涂层的试样 ADH：完成粘附性能测试后涂覆壳聚糖/生物活性玻璃涂层的试样 SBF：在模拟体液（Simulated Body Fluid，SBF）中完成生物活性测试后的试样 SEM：扫描电子显微镜（Scanning Electron Microscopy，SEM） EDS：能量色散谱（Energy Dispersive Spectroscopy，EDS） 各文件夹包含内容如下： Corrosion（腐蚀测试文件夹）：包含电化学测试得到的耐腐蚀性能相关数据文件 FTIR（傅里叶变换红外光谱文件夹）：包含壳聚糖/生物活性玻璃涂层的傅里叶变换红外光谱分析所得文件 Roughness（表面粗糙度文件夹）：包含利用光学轮廓仪针对不同扫描区域得到的表面形貌分析文件 SEM（扫描电子显微镜文件夹）：包含各类试样表面的扫描电子显微镜成像文件，其子文件夹包括： Adhesion（粘附性能测试组）：包含胶带剥离测试后涂覆壳聚糖/生物活性玻璃涂层的试样的SEM图像 Bioactivity test（生物活性测试组）：包含在SBF中完成生物活性测试后涂覆壳聚糖/生物活性玻璃涂层的试样的SEM图像及EDS分析结果 Coatings（涂层组）：包含沉积于不同基底上的壳聚糖/生物活性玻璃涂层的SEM图像 Substrate（基底组）：包含经各类表面改性处理后的钛基底的SEM图像 Wettability（润湿性能测试文件夹）：包含润湿性能测试所得的相关数据文件 XRD（X射线衍射文件夹）：包含X射线光谱分析所得的相关数据文件 本研究由波兰国家科学中心（National Science Centre, Poland）基于OPUS 23号项目[2022/45/B/ST5/03398]资助。