The data of RPhC, TLC, and MALDI analysis of molecular masses of fluorescent ligopeptides forming after incubation of X-OP25 with sle-IgGmix.
收藏资源简介:
*Free fluorescent compound; all analyzed OPs contained fluorescent X-component.**The same products of the hydrolysis separated by RPhC (Fig. 5A) were revealed in several peaks by MALDI spectrometry; the main peaks are marked in bold, while additional peaks are shown in parentheses. C1 reflects the presence of signal corresponding to the analyzed product in the spectrum of total reaction mixture.***The same several products of the hydrolysis corresponding to each peak after RPhC (Fig. 5A) were revealed not only by MALDI spectrometry, but also by TLC (Fig. 5B)
*游离荧光化合物;所有分析的有机磷化合物(Organophosphorus compounds, OPs)均含有荧光X组分。**经反相液相色谱(Reversed-Phase Chromatography, RPhC)分离得到的水解产物(图5A),经基质辅助激光解吸电离质谱(Matrix-Assisted Laser Desorption/Ionization Mass Spectrometry, MALDI)检测到多个信号峰;主峰以粗体标注,副峰以括号标注。C1代表总反应混合物质谱谱图中与目标分析产物对应的信号存在情况。***经反相液相色谱分离后与各峰对应的水解产物(图5A),不仅可通过基质辅助激光解吸电离质谱检测到,也可通过薄层色谱(Thin Layer Chromatography, TLC)观测到(图5B)。*



