Synthesis of Substituted Trinaphthylenes
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https://figshare.com/articles/dataset/Synthesis_of_Substituted_Trinaphthylenes/2092711
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资源简介：
A short
synthesis of six trinaphthylenes is reported. The cyclotrinaphthylenes
carry six alkoxy groups, and derivatives featuring OHex, OBu, OiPr,
OPr, OEt, and OMe substituents can be obtained by an ordinary Ni(COD)2-promoted, Yamamoto-type coupling reaction. Cyclotrimerization
yields range from 38% to 65%. Dependent upon their structure, the
cyclotrinaphthylenes assume different packing patterns, according
to single-crystal X-ray structure determination. The crystal structures
of such trinaphthylenes were hitherto undescribed.
创建时间：
2016-02-12
