XRD raw data of new pertechnetate compounds

Datasets of XRD measurements of [Pr(TcO4)3(H2O)3] and [Sm(TcO4)3(H2O)3]. CYTc8.zip is a dataset for [Sm(TcO4)3(H2O)3]. CYTc36.zip and CYTc41_new.zip are datasets for [Pr(TcO4)3(H2O)3] Both datasets show twinning which could not be modelled satisfactorily yet. If you are able to solve the structure, please contact [e-mail]针对[Pr(TcO4)3(H2O)3]与[Sm(TcO4)3(H2O)3]的X射线衍射（X-ray Diffraction, XRD）测量数据集。 CYTc8.zip 为针对[Sm(TcO4)3(H2O)3]的数据集。 CYTc36.zip 与 CYTc41_new.zip 则为针对[Pr(TcO4)3(H2O)3]的数据集。 上述两类数据集均存在孪晶现象，目前尚未能得到令人满意的建模解析。 若您能够解析该晶体结构，请联系 [e-mail]