Data for: Recyclable supported Pd-NHC catalytic systems for the copper-free Sonogashira cross-coupling under continuous flow

Experimental procedure for the immobilisation of recyclable catalytic systems is described. TGA data for the silica, alumina and titania supported catalyts is given. Experimental procedure for optimization and performance of Sonogashira reaction in bathc and under continuous flow using supported catalysts is described. Recyclability experiments are described. Sonogashira coupling products data is reported along with the corresponding NMR spectra.

本文详细描述了可回收催化体系的固定化实验流程。提供了二氧化硅、氧化铝及二氧化钛负载型催化剂的热重分析（Thermogravimetric Analysis, TGA）数据。同时详述了采用负载型催化剂，在间歇式与连续流条件下开展Sonogashira反应的优化及性能评价实验流程。此外还介绍了可回收性实验的相关内容，并报道了Sonogashira偶联产物的相关数据及其对应的核磁共振波谱（Nuclear Magnetic Resonance, NMR）。