Thermal behaviour of ammonium vanadate nanocrystals

The DataSet contains the thermal behavior of the ammonium vanadate nanostructures obtained by the hydrothermal method with different conditions. Thermogravimetric analysis (TG) was carried out under an argon atmosphere from 40C to 560C (with a heating rate of 10 C/min) using Netzsch STA 449 F1. The thermal behavior was also studied with mass spectrum (MS). The gases that come out from the samples during heating were monitored by the quadruple mass spectrometer Netzsch QMS 403C Aeolos. The mass spectra were measured from m/z 2 to 60. The results reveal the differences in registered ion currents. 
These results are part of a project defined in Electrochimica Acta journal (10.1016/j.electacta.2020.135919). In this paper, the information about samples and synthesis details are reported.

本数据集收录了通过水热法制备、不同实验条件下合成的钒酸铵纳米结构的热行为数据。本研究采用耐驰（Netzsch）STA 449 F1型热重分析仪，在氩气氛围下以10℃/min的升温速率，于40℃至560℃区间内完成了热重分析（Thermogravimetric Analysis, TG）；同时借助质谱（Mass Spectrum, MS）对该热行为展开研究。加热过程中样品逸出的气体，通过耐驰QMS 403C Aeolos型四极杆质谱仪（Quadrupole Mass Spectrometer）进行监测，质谱检测范围为质荷比（m/z）2至60。实验结果揭示了各测试条件下记录的离子电流存在差异。
本数据集的相关结果隶属于发表于《Electrochimica Acta》期刊（DOI: 10.1016/j.electacta.2020.135919）的研究项目，该论文详细记载了实验样品的相关信息与合成工艺细节。