Dataset of report: A221 Validation of the protocol developed in A2.1.4 by demonstrating its applicability for siloxanes

IMBiH, NPL, VSL and RISE have each validated the fitness of purpose of the performance assessment protocol developed in A2.1.4 by demonstrating its applicability for total silicon using a range of different atomic/ionic emission spectrometry-based analysers and for individual siloxanes (siloxanes: L2, L3, D3, D4, D5) using thermal desorption gas chromatography mass spectrometry flame ionization detector (TD-GC/MS/FID) at VSL and RISE, and GC-IMS at NPL. RISE, IMBiH, VSL and NPL will use the gravimetrically prepared static standards produced in A1.1.2 and A1.1.3.

IMBiH、NPL、VSL与RISE四家机构均已完成对A2.1.4中开发的性能评估协议的适用性验证：通过采用多款基于原子/离子发射光谱法的分析仪开展总硅检测，证实了该协议在总硅检测中的适用性；针对单体硅氧烷（siloxanes），包括L2、L3、D3、D4、D5，VSL与RISE采用热脱附气相色谱-质谱/火焰离子化检测器（TD-GC/MS/FID）完成验证，NPL则通过气相色谱-离子迁移谱（GC-IMS）完成验证。RISE、IMBiH、VSL及NPL四家机构将采用A1.1.2与A1.1.3中通过重量法制备的静态标准物质。