新型芳基脂肪酸酰胺叔胺类表面活性剂制备技术生产示范数据集

在建成的年产1000吨的生产示范装置上，完成反应及检测，得到相应的结果。涉及到原料检测，工艺过程中的检测，不同平行反应器中的转化率检测，不同时间点的检测。气相色谱采用上海舜宇恒平科学仪器有限公司的气相色谱仪（型号GC-1290，配备自动进样器）和M6色谱工作站采集；液相色谱采用上海伍丰科学仪器有限公司的液相色谱仪（型号LC-100 Plus，配备自动进样器）和相应色谱工作站采集；质谱使用日本岛津公司的液质联用仪（型号LC-MS/MS 8045）及相关工作站采集集；界面张力测定采用上海地学仪器研究所的旋转滴界面张力仪（TX-500C）测定。数据量19.4 MB。Reactions and testing were conducted on the commissioned 1,000-ton-per-year production demonstration plant, and corresponding results were obtained. The testing covers raw material inspection, in-process detection, conversion rate testing in different parallel reactors, and detection at various time points. Gas chromatography data was collected using a gas chromatograph (model GC-1290, equipped with an autosampler) and the M6 chromatography workstation from Shanghai Sunny Hengping Scientific Instruments Co., Ltd. High performance liquid chromatography data was collected using a liquid chromatograph (model LC-100 Plus, equipped with an autosampler) and the corresponding chromatography workstation from Shanghai Wufeng Scientific Instruments Co., Ltd. Mass spectrometry data was collected using a liquid chromatography-tandem mass spectrometry (LC-MS/MS 8045) system and its associated workstation from Shimadzu Corporation of Japan. Interfacial tension was measured using a spinning drop interfacial tensiometer (model TX-500C) from Shanghai Geological Instruments Research Institute. The total data size of this dataset is 19.4 MB.

搜集汇总

背景与挑战

背景概述

该数据集基于年产1000吨的生产示范装置，采集了新型芳基脂肪酸酰胺叔胺类表面活性剂制备过程中的原料、工艺、转化率及时间点检测数据，使用气相色谱、液相色谱、质谱和界面张力仪等设备，数据量为19.4 MB。