Facile Synthesis of the Tridecameric Al<sub>13</sub> Nanocluster Al<sub>13</sub>(μ<sub>3</sub>-OH)<sub>6</sub>(μ<sub>2</sub>-OH)<sub>18</sub>(H<sub>2</sub>O)<sub>24</sub>(NO<sub>3</sub>)<sub>15</sub>
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Treatment of aluminum nitrate with an organic nitroso-containing compound yields the “flat”, tridecameric nanocluster Al13(μ3-OH)6(μ2-OH)18(H2O)24(NO3)15 (Al13) in good yield on a preparative scale under ambient conditions. Synthetic procedures yielding two different single-crystal forms of the Al13 cation with two varying counterion compositions are described.
创建时间：
2008-02-18
